Updated 21st Sep. 2017






















Permanent Organisers



by E.J. Watkinson
2017


by Y. Zhang and C. Esling
2015


by S. Alleg and S. Ouhenia
2012


by M. Zucali and M. Dapiaggi
2009

Local Organisers



2016-2020



2013-2014
Financing partners








Partners




Workshop series on Combined Analysis using x-rays, neutrons and electron scattering


Organisers:
Luca Lutterotti, Giancarlo Pepponi: University of Trento and Fondazione Bruno Kessler, Italia
Daniel Chateigner, Magali Morales, Stephanie Gascoin: Normandie Universite, Universite Caen Normandie and CNRS
Eric Berthier, Christophe Fontugne, Henry Pilliere: Thermo Fisher Scientific


Why not a New session at your place ?! Next ones:
December 2017, Shenyang, China: a small session
July 2018, Caen, France
October 2018, Trento, Italia


Prerequisites
Crystallography basics
(Magali Morales)

in French
Prerequisites (S. Enzo) X-ray Diffraction - Basics
(Magali Morales)
Introduction Crystallography, Diffraction Techniques
Luca Lutterotti

Rays-Matter Interactions
(Giancarlo Pepponi 2015)



Courses
Technical Issues (Henry Pilliere)
2017 2016 2015 2010
Rietveld Analysis (L. Lutterotti)
2017 2016 2015 2013 2010
Quantitative Texture Analysis (Daniel Chateigner)
2017 2016 2015 2014
QTA under High-pressure (Hans-Rudolf Wenk 2015)
Microstructure Analysis (Daniel Chateigner)
Microstructure (L. Lutterotti)
2017 2016 2015
Planar defects (L. Lutterotti)
Residual Stress Analysis (L. Lutterotti)
2016 2015 2013 2010
Quantitative Phase Analysis (L. Lutterotti)
Reflectivity Analysis (Daniel Chateigner)
X-Ray Fluorescence (Christina Streli 2015)
X-Ray Fluorescence Fundamentals (Giancarlo Pepponi)
2017 2016
XRR and GIXRF (Giancarlo Pepponi)
2016 2015
Combined XRD-XRR-XRF (Luca Lutterotti)
2017
Analytical Electron Microscopy
(Stefano Gialanella, 2015)

Electron Diffraction Patterns
(Philippe Boullay)

2016 2015
Pair Distribution Function (L. Lutterotti)
2016


Combined Analysis (D. Chateigner)
Combined Analysis from Images (L. Lutterotti)
2016 2015
Aperiodic Structures (D. Grebille, †2009)
Application to films (M. Morales)

Some Tools
Crystallography
Open Database (COD)

Structure Databases (L. Lutterotti) Collection Strategies (L. Lutterotti) Material Properties
Open Database (L. Fuentes, D. Chateigner, G. Pepponi, S. Grazulis)

The MAUD page
Dropbox Newest versions
OS X v2.74, 2017-06-30
Windows 2016-06-28
Windows 64b 2016-06-28
Unix 2016-06-28
Unix 64b 2016-06-28
MAUD.jar version 2015-10-21
Install MAUD
Video (L. Lutterotti)

Phase Id by
Full-Pattern Search-Match on Internet
Caen mirror -- Trento mirror
Theoretically optimized COD
Predicted COD
Raman
Open Database

X-ray database for MAUD (oct. 2015)
MAUD Forum
MAUD Twitter


Exercises




Instrument calibrations
LaB6 standard, instrumental function
Tutorial (M. Morales)
LaB6 standard, misaligned instrument
Al2O3 neutron standard
Y2O3 CPD round Robin
One phase, isotropic size

The Aluminum Random Texture Standard
sample from Labotex
The Aluminum Orthorhombic Texture Standard
sample from Labotex
The Aluminum Triclinic Texture Standard
sample from Labotex
APS synchrotron image (CeO2)
(Hans-Rudolf Wenk)

APS synchrotron image (LaB6)
(Hans-Rudolf Wenk)

Quantitative Phase Analysis (QPA)
ZnO/Al2O3/CaF2 mixture (CPD round robin)
Multiphase, isotropic size




Quantitative Microstructure Analysis (QMA)
TiO2 nanopowder
X-rays Anisotropic sizes

Faujasite X
Isotropic size + Pattern Matching
EMT Zeolite nanopowderAnisotropic size + Pattern matching

QPA + QMA
Al2O3 + Ce-ZrO2
QPA + anisotropic QMA

Cr-Ni steel
QPA + anisotropic QMA

alpha + beta brass
QPA with size distributions

Irradiated Fluorapatite
QPA Amorphous + crystalline phases

SiO2 + Al2O3
QPA Amorphous + crystalline phases

Brucite/Aragonite powder
X-rays Anisotropic sizes

bcc/fcc Fe-Cr-Mo steels
QPA + anisotropic sizes
Shale
(Hans-Rudolf Wenk)

Quantitative Texture Analysis (QTA)
Uniaxially aligned aragonite bulk
QTA planar texture

Centrifugated mullite needles
QTA planar texture

gamma-TiAl
neutron QTA: grain statistics problem

Co-349 bulk
Neutron Texture + incommensurate supercell

Cu-Fe alloys
Neutron TOF QTA

PCT/Pt bilayer
X-ray QTA + layering

W rolled bulk
x-rays, CPS120

Quartzite
TOF neutrons, HIPPO
(Hans-Rudolf Wenk)

QTA + QPA
m-ZrO2 + t-ZrO2 bulk
neutron QTA, polyphased




QTA + QMA
nano-TiO2 ring patterns
Electron Diffraction

Tutorial (Philippe Boullay)



QTA + Residual Stresses Analysis (RSA)
Ca-ZrO2 film
X-ray QTA + residual stresses




QTA + QMA + Residual Stresses Analysis (RSA)
AlN/Pt/Ni-Co-Cr-Al stack
x-rays, CPS120

BST(3000 nm)/Al2O3 substrate
x-rays, CPS120

BST(250 nm)/Pt(120 nm)
x-rays, CPS120

MgFeO in diamond anvil cell
APS synchrotron image
(Hans-Rudolf Wenk)
QTA + QMA + RSA + Structure Refinement (SR)
PZT(200 nm)/LNO(40 nm) bi-layer
x-rays, CPS120



QTA + QMA + RSA + SR
ITO film
x-rays, CPS120



X-Rays specular Reflectivity (XRR)
SiO2/Si
XRR

other XRR





X-Ray Fluorescence (XRF) and Diffraction
PbTiO3





XRR + Grazing Incidence XRF (GIXRF)
Ti film





XRD + XRF + XRR
Example





Rietveld + Pair Distribution Function (PDF)
InGaN





Other utilities
ODF refinement from measured pole figures
Tutorial (L. Lutterotti)
EDP Tutorial
(Philippe Boullay)

Synchrotron Images Part I
(Luca Lutterotti)

Synchrotron Images Part II
(Hans-Rudolf Wenk)

Batching analyses (FeCu)
Tutorial (L. Lutterotti)








References
Bunge, H.-J. (1993): Texture Analysis in Material Science: Mathematical Methods
Matthies, Vinel, Helming (1987): Standard Distributions in Texture Analysis


Pictures
2017 One-day Introduction, Leicester 2017 Workshop, Caen
Program
Participants
Agenda


2016 Workshop, Caen
Program
Participants
Agenda
2015 Workshop, Trento
Program
2015 During Texture and Anisotropy meeting, Metz
2014 Workshop, Caen
Program
Participants
Agenda
2013 Workshop, Caen
Program
Participants
Agenda
2012 Workshop, Annaba
Program
Agenda
2012 During Texture and Anisotropy meeting, Caen
2011 Workshop, Caen
Program
Participants
Agenda
2010 Workshop, Caen
Program
Participants
Agenda
2009 Texture Workshop, Milano
Program
Agenda





Comments and suggestions are very welcome
© 2000 - All rights reserved daniel dot chateigner at ensicaen dot fr